Laboratories

The laboratories that support ongoing work in the PPGEMN are divided between those of the School of Engineering and MackGraphe. The infrastructure of all these laboratories is detailed on their pages in the PNIPE – National Platform for Research Infrastructure, from the MCTI, with links provided below.

All laboratory infrastructure, both from MackGraphe and the School of Engineering, is available to the entire academic-scientific community, both internal and external to UPM, through Mackenzie's multi-user laboratory policies (https://www.mackenzie.br/mack-laboratorios-multiusuarios/home)

LPCM

A complex of laboratories at the School of Engineering, covering the three main areas of Materials Engineering – metallic, ceramic, and polymeric materials. It is divided into the following specific laboratories:

Materials Characterisation Lab
Polymer Materials Processing Lab
Surface Techniques Lab
X-ray Techniques Lab
ZwickRoell – Mackenzie Space
Netzsch-Mackenzie Space
Ceramic Materials Processing Lab
Foundry Lab

It aims to characterise polymeric, ceramic, metallic, and composite materials. Main equipment:

  • Ultra Digital Dynamic Microhardness Tester (Shimadzu DUH-211S)
  • UV-VIS Spectrophotometer (Shimadzu, UV-2600)
  • Freeze Dryer (Terroni, LS series)
  • Zeta Potential and Particle Size Analysis Equipment by DLS (Anton Paar, Litesizer 500)
  • Dynamic Mechanical Analyzer (Perkin Elmer, DMA 8000)
  • Sputter Coater (Baltec, SCD050)
  • Scanning Electron Microscope (JEOL, JSM-6510)
  • Impact Testing Machine with low-temperature testing accessory (down to -60ºC) (Tinius Olsen, IT 504)
  • Accelerated Ageing Chamber (Q-Lab, QUV/spray)
  • Shott Viscometer Sets
  • Atomic Absorption Spectrometer (Varian, AA1275)
  • Thermal Deflection (HDT and VICAT) (Tinius Olsen, HD94/398)
  • SUSSEN Hardness Tester (15 to 250 kg) (Testor, HRB and HRC)
  • Universal Testing Machine (Zwick Roell)
  • Digital Impact Testing Machine (Tinius Olsen, 892)
  • Precision Cutter, 50 – 1500 rpm (Pace Technologies, Pico 155)
  • Horizontal Tubular Furnace (EDG, EDG10P-S)
  • ​​​​​​​Optical Microscope (Olympus, BX60M)

It aims to process thermoplastic polymer materials and their composites. Main equipment:

  • Calender (Mecanoplast, C400-3)
  • Thermoforming Machine (Brawel, VF BPP 30x36)
  • Banbury (Closed Mixer)
  • Agglomerator (KIE, AK40)
  • Thermoplastic Injection Moulding Machine (ROMI Primax, 65R)
  • Thermostatic Bath (FANEM)
  • Reactor (Metler Toledo, Labmax)
  • Rheometer (Haake, Reodrive 5000)

 

The Surface Techniques Lab is dedicated to studies related to the surface of materials, corrosion, thin film deposition, and surface modification using plasma. Key equipment:

  • Microscratch and Microindenter (Anton Paar MCT³);
  • High-temperature tubular furnace with atmosphere control.

This lab brings together equipment for characterization based on X-rays. Key equipment:

  • X-ray Diffractometer (Rigaku);
  • X-ray Fluorescence (Oxford X-SUPREME 800).

Inaugurated in 2022, this laboratory is the result of a cooperation agreement and joint investment between UPM and the German company ZwickRoell. It is dedicated to teaching, research, service provision, and other activities carried out in collaboration with partner companies and the community. Key equipment:

  • Electromechanical Creep Testing Machine (Zwick Roell, Kappa 10DS);
  • Universal Testing Machine (Zwick Roell);
  • Aflow Flowability Testing Equipment (Property of ZwickRoell – On loan);
  • DuraScan 80 Microhardness Tester (Property of ZwickRoell – On loan);
  • Rockwell ZHR Indentec Hardness Tester (Property of ZwickRoell – On loan);
  • Shore D Durometer (Property of ZwickRoell – On loan).

Inaugurated in 2024 as a result of a cooperation and joint investment between UPM and the German company Netzsch, this laboratory is dedicated to teaching, research, service provision, and other activities carried out in collaboration with partner companies and the community. Key equipment:

  • Thermal Analysis (Netzsch STA 409);
  • Thermal Analysis (Netzsch DSC Carilis 300) (Property of Netzsch – On loan);
  • Dynamic Mechanical Thermal Analysis (Netzsch DMA 242E Artemis) (Property of Netzsch – On loan);
  • Dilatometer (Netzsch DIL 402 Expedis Classic) (Property of Netzsch – On loan);
  • Oscillatory Rheometer (Netzsch Kinexus pro) (Property of Netzsch – On loan).

 

This laboratory is dedicated to operations involving pressing, extrusion, and bonding, and also includes furnaces with medium (up to 1200°C) and high (up to 1700°C) temperatures. Key equipment:

  • Extruder (Verdés, BR 051);
  • Oven (Fanem, 315 SE);
  • Filter Press (Rexroth);
  • Muffle Furnace (1200°C) Programmable Digital;
  • LF1700°C Furnace - Manufacturer Jung;
  • Pot Turner (Gardelin, 4162).

This laboratory is aimed at the heat treatment of metallic materials and processes involving casting operations, as well as the design, sizing, and execution of sand casting molds. Key equipment:

  • 2 Heat Treatment Furnaces, Temperature up to 1300°C (Brasimet);
  • Crucible Casting Furnace with control panel (Inductotherm);
  • Centrifugal casing for obtaining centrifugally cast tubes (Magneti Marelli – Cofap).

LPsQ

It has infrastructure and analytical instrumentation for the development of activities related to the synthesis, functionalization, and characterization of nanostructures and nanomaterials. Key equipment:

Nuclear Magnetic Resonance (NMReady, 60 Pro);
Atomic Absorption - Flame and Graphite Furnace (Analytik Jena, Contraa 700);
Autoclave (Quimis);
Centrifuge (Centribio, 80-2B);
Conductivity Meter (Digimed, DM-32);
Ion Chromatograph (Metrohm, 792 Basic IC);
Gas Chromatograph (Agilent, 5890 Series II);
2 High-Performance Liquid Chromatographs (HPLC) (Dionex and Agilent);
Sample Digester;
UV-Vis Spectrophotometer (Shimadzu, UV-1601);
Infrared Spectrometer (Shimadzu, IRAffinity-1);
Vacuum Oven (Tecnal, TE-395);
Lyophiliser;
Knife Mill (Solab Cientifica, SL 31);
Reverse Osmosis (Gehaka, OS50 LX);
Magnetic Stirring Plate (Fisatom, 751);
Potentiostats (Metrohm, PGStart 128N & 204);
Rotavapor (Buchi, R-100);
Tip Ultrasonic (Eco-sonics);
Water Baths, Ultrasonic Baths, and Stirring Tables.


LabNAHM

It has infrastructure and analytical instrumentation for the development of nanostructures and nanomaterials for electrochemical sensors and nanofiltration systems. Key equipment includes:

Potentiostats/Galvanostats (Autolab, models: PGSTAT12 [1 unit]; PGSTAT302N [2 units]);
Potentiostat/Galvanostat with Electrochemical Spectroscopy (Autolab, PGSTAT204, modules: LIGHT SOURCE and SPECTROPHOTOMETER-UA);
Glove Box (MBraum, GB 2202 P-VAC);
Vacuum Oven (Tecnal, TE-395);
Digital Sterilisation and Drying Oven (SolidSteel, SSDi-40L);
3D Resin Printer with Wash and Drying Tank (Anycubic, Photon Mono M5s);
Vortex Mixer (ION, VX-38);
2 UV-Vis Spectrophotometers (Agilent and Thermo);
3D Filament Printer (Core A3, GT MAX 3D);
Centrifuge (FANEM, 206);
MALDI Mass Spectrometer (Thermo Fisher).


MackGraphe Laboratories

Multidisciplinary Facility with Emphasis on Nano/Microelectronics and Nanophotonics. This facility is designed for the development, production, and characterization of nanomaterial-based devices. It is equipped with state-of-the-art infrastructure in a cleanroom environment (Class 1000 and 100) spanning 180 m². The laboratory focuses on research and development in nanoelectronics, microelectronics, and nanophotonics.

Key Equipment:

  • CVD System for graphene and other 2D materials growth (Graphene Square TCVD-50B);
  • Semi-Automatic Wire Bonder (for micro-soldering);
  • Reactive Ion Etching (RIE) Equipment (Oxford, PlasmaPro 80);
  • UV-Vis-NIR Spectrophotometer (Shimadzu, UV-Vis-NIR 3600 Plus);
  • Scanning Electron Microscope (JEOL, JSM-7800F) with: microammeter, nanometer pattern generation system, and X-ray microanalysis system;
  • Atomic Force Microscope (AFM) (Bruker, Dimension Icon);
  • Direct Write Optical Lithography System (Durham, MicroWriter ML3 Baby);
  • Wirebonding Microsoldering System (TPT, HB10);
  • Atomic Layer Deposition (ALD) (ANRIC AT410) with ozone generator;
  • Electron Beam Deposition System (E-BEAM) (M-Braun MB-ProVap).

This facility supports cutting-edge research and development in the fields of nanoelectronics and nanophotonics, providing high-end tools for material research and device fabrication. It is open to academic, scientific, and industrial collaborations for both fundamental and applied research in nanotechnology.

 

 

Research and Development laboratory set focusing on the synthesis and characterization of nanomaterials and innovations in nanostructured and multifunctional materials. Key equipment:

  • Bench Scanning Electron Microscope (Hitachi, TM-3000);
  • X-ray Photoelectron Spectrometer (XPS) (Thermo Fisher, K-alpha);
  • High-resolution Inverted Confocal Microscope (Olympus-Visitech);
  • Glove Box with six gloves and Argon environment (MBraun);
  • FTIR and microFTIR Spectrometer (Bruker, Vertex 70 and Hyperion II);
  • Semiconductor Parameter Analyzer (Keysight, B1500A) + Analytical Probe Station (Signatone, H150W);
  • Confocal Raman Microscopy System, with laser lines at 488nm, 532nm, and 633nm (WITec Alpha 300R);
  • UV-Vis-NIR Spectrophotometer (Shimadzu, UV-Vis-NIR 3600 Plus);
  • Particle Size Analyzer – DLS and Zeta Potential (Anton Paar, Litesizer 500);
  • X-ray Diffractometer (Bruker, D8 Advance);
  • Bench Thermoplastic Extruder (Thermo Scientific, Process11);
  • Impact Testing Machine (Tinius Olsen, IT 504);
  • Planetary Centrifugal Mixer (MTI Group, MSK-PCV 300);
  • Plasma Prep Etcher (SPI Supplies, 11050);
  • Surface Zeta Potential Analyzer (Anton Paar, Surpass 3);
  • 3 Potentiostats/Galvanostats equipped with Impedance Module and Current Booster (Autolab Metrohm);
  • Simultaneous TGA/DSC Thermal Analyzer (TA Instruments, SDT-Q600);
  • Modular Cycler for Coin-cell 50mA – 5V (Neware);
  • Differential Scanning Calorimeter (Shimadzu, DSC-60 Plus);
  • Twin-screw Extruder (Thermo Scientific, TSE 24);
  • Compact Modular Rheometer (Anton Paar, MCR 702 MultiDrive);
  • Size Exclusion Chromatography (CET) with Refractive Index Detector and operation at temperatures up to 150°C (Viscotek, HT-GPC 350A);
  • Contact Angle Analyzer with Temperature-Controlled Chamber up to 400°C (Kruss, DSA 100B);
  • HAAKE Injection Molding System (Thermo Scientific, Minijet Pro).

 

Optics and Photonics Laboratory Set for Optical Characterisation of 2D Materials and Development of Photonic Devices Using Nanomaterials for Telecommunications and Sensing. Main Equipment:

  • Optical parametric amplifier with pulse compressor, fibre laser pumped, generating pulses <90 fs in the 650-920 nm (signal) and 1150-2500 nm (idler) ranges (Amplitude, Satsuma HP + Mango SP + compressor);
  • Modular laser system providing 100 fs pulses at 1550 nm, supercontinuum spectrum, and 30 fs pulses tunable between 1000 and 1400 nm (Toptica, FFS.SYS.COMP);
  • Single-mode fibre lasers and amplifiers with powers up to 4W;
  • 1 High-power supercontinuum source covering the 400-2400 nm range (NKT, SuperK EXTREME EXB-1);
  • Tunable laser from 3800 to 4800 nm (IPG Photonics, FLT-4350/1100-0.1, Fe:ZnSe);
  • Solid-state mid-infrared laser, tunable in the 2-3 μm range (IPG Photonics, NLTL-Cr: ZnS / Se-2500-1000-100);
  • 3 optical spectrum analysers covering the visible and near-infrared (Yokogawa and Agilent);
  • Optical frequency domain reflectometer (Luna, OBR 30m);
  • Optical Cryostat System (Cryofab, CMSHSS100);
  • Optical beam profiler in the visible, near-infrared, and 1550 nm ranges (Newport);
  • Simulation and analysis software (Comsol Multiphysics, VPI Transmission Maker, Matlab);
  • 59 GHz Oscilloscope (Keysight, DSOZ592A);
  • Spectrum analyser up to 44 GHz (Keysight, N9951A).

R&D Laboratory Set Focused on Innovation in Nanobiotechnologies, Including Biosensors and Use of Mass Spectrometry for Various Applications, Both in Health and Other Areas. Main Equipment:

  • Mass spectrometer with Plate Express® TLC Plate Reader (Atmospheric Solids); Analysis Probe (ASAP), inert Atmospheric Solids Analysis Probe (iASAP), Touch Express™ Open Port Sampling Interface (OPSI), and Volatile APCI (vAPCI) (Advion, Expression CMS);
  • Mass spectrometer with ambient ionisation source EASI and UFswitching and UFscanning (Shimadzu, LC-MS 2020);
  • Mass spectrometer with 2D imaging system, moving stage and Omni Spray (Thermo Scientific, Ion Trap 3D);
  • Mass spectrometry pen for cancer detection (Genio Technology, MassSpec Pen Preciso™);
  • Orbitrap MALDI Mass Spectrometer (Thermo Scientific, Qexactive);
  • Trinocular Inverted Microscope (Evident/Olympus, CKX53);
  • 3D Extrusion Bioprinter (TissueLabs, TissueStart);
  • 3D Stereography Bioprinter (TissueLabs, TissueRay);
  • Cell Counter (Thermo Fisher Scientific, Countess™ 3);
  • UV-Vis Microplate Spectrophotometer (Thermo Scientific, Multiskan SkyHigh);
  • Bacteriological Incubator (Tecnal, TE-392/93L);
  • CO2 Incubator (Thermo Scientific, 4111);
  • IoT Radiocommunication Tester (Rohde & Schwarz, CMW290);
  • Anechoic Chamber (Rohde-Schwarz, DTS 200).